A 20μl aliquot of the resulting solution was injected into the LC/MS/MS system for analysis.Those plasma samples whose concentrations were greater than the upper limit of quantification (ULOQ) were diluted appropriately with blank plasma to adjust the concentration to within the range of the standard curve before sample preparation,and then reanalyzed.
将20μl合成溶液注入LC / MS / MS系统,进行分析.这些等离子体样品的浓度大于上限量化(ULOQ),与空白血浆适当稀释以调整浓度,并在制备样品前使浓度值处于标准曲线范围之内,之后可重新分析.